Information card for entry 7028880

Structure parameters

• Formula: C35 H34 Cl2 O2 P2 Pd S2
• Calculated formula: C35 H34 Cl2 O2 P2 Pd S2
• Title of publication: Oxidative addition chemistry of tetrathiocines: synthesis, structures and properties of group 10 dithiolate complexes.
• Authors of publication: Wrixon, Justin D.; Hayward, John J.; Raza, Osman; Rawson, Jeremy M.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2014
• Journal volume: 43
• Journal issue: 5
• Pages of publication: 2134 - 2139
• a: 20.866 ± 0.0021 Å
• b: 20.866 ± 0.0021 Å
• c: 15.5435 ± 0.0016 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 6767.5 ± 1.2 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 7
• Space group number: 122
• Hermann-Mauguin space group symbol: I -4 2 d
• Hall space group symbol: I -4 2bw
• Residual factor for all reflections: 0.0325
• Residual factor for significantly intense reflections: 0.0289
• Weighted residual factors for significantly intense reflections: 0.0666
• Weighted residual factors for all reflections included in the refinement: 0.0688
• Goodness-of-fit parameter for all reflections included in the refinement: 1.064
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No