Information card for entry 7029046

Structure parameters

• Formula: C104 H86 N16 O34 P4 Sn6
• Calculated formula: C104 H86 N16 O34 P4 Sn6
• SMILES: c1(c(cccc1)/N=N/c1ccccc1)[Sn]1234OP5(=[O][Sn]67([O]1[Sn]1(O6)(O5)([O]=P(O3)(O[Sn]356([O]=P8(O[Sn]9(c%10ccccc%10/N=N/c%10ccccc%10)([O]=P(O[Sn](O8)([O]39)(c3ccccc3/N=N/c3ccccc3)(O6)O4)(O7)Oc3ccc(N(=O)=O)cc3)(O5)O1)Oc1ccc(N(=O)=O)cc1)c1ccccc1/N=N/c1ccccc1)Oc1ccc(N(=O)=O)cc1)c1ccccc1/N=N/c1ccccc1)(c1ccccc1/N=N/c1ccccc1)O2)Oc1ccc(N(=O)=O)cc1.C1OCCC1.C1CCCO1
• Title of publication: Assembly of hexa- and trinuclear monoorganostannoxanes: hemi-labile nature of intramolecular N→Sn coordination in RSnCl3 (R = 2-phenylazophenyl).
• Authors of publication: Metre, Ramesh K.; Mohapatra, Chandrajeet; Sahoo, Dipankar; Chandrasekhar, Vadapalli
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2014
• Journal volume: 43
• Journal issue: 8
• Pages of publication: 3364 - 3371
• a: 13.185 ± 0.005 Å
• b: 14.386 ± 0.005 Å
• c: 16.439 ± 0.005 Å
• α: 105.986 ± 0.005°
• β: 100.34 ± 0.005°
• γ: 94.817 ± 0.005°
• Cell volume: 2919.4 ± 1.7 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1369
• Residual factor for significantly intense reflections: 0.0795
• Weighted residual factors for significantly intense reflections: 0.1834
• Weighted residual factors for all reflections included in the refinement: 0.2162
• Goodness-of-fit parameter for all reflections included in the refinement: 0.966
• Diffraction radiation wavelength: 0.71069 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No