Information card for entry 7029269

Structure parameters

• Formula: C60 H45 B F24 N4 O5.5 Rh
• Calculated formula: C60 H44 B F24 N4 O5.5 Rh
• Title of publication: Ring expansion of a 2-rhodaoxetane: insertion chemistry with unsaturated molecules.
• Authors of publication: Desnoyer, Addison N.; Dauth, Alexander; Patrick, Brian O.; Love, Jennifer A.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2014
• Journal volume: 43
• Journal issue: 1
• Pages of publication: 30 - 33
• a: 9.5642 ± 0.0013 Å
• b: 18.249 ± 0.002 Å
• c: 19.551 ± 0.003 Å
• α: 116.345 ± 0.003°
• β: 96.706 ± 0.004°
• γ: 91.811 ± 0.004°
• Cell volume: 3023.7 ± 0.7 ų
• Cell temperature: 90 ± 2 K
• Ambient diffraction temperature: 90 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0593
• Residual factor for significantly intense reflections: 0.0474
• Weighted residual factors for significantly intense reflections: 0.1183
• Weighted residual factors for all reflections included in the refinement: 0.1242
• Goodness-of-fit parameter for all reflections included in the refinement: 1.033
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No