Information card for entry 7029289

Structure parameters

• Formula: C56 H89 Cl Ge N2 Si2
• Calculated formula: C56 H89 Cl Ge N2 Si2
• Title of publication: NHC-coordinated silagermenylidene functionalized in allylic position and its behaviour as a ligand.
• Authors of publication: Jana, Anukul; Majumdar, Moumita; Huch, Volker; Zimmer, Michael; Scheschkewitz, David
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2014
• Journal volume: 43
• Journal issue: 13
• Pages of publication: 5175 - 5181
• a: 20.3816 ± 0.0011 Å
• b: 10.9027 ± 0.0006 Å
• c: 25.5288 ± 0.0013 Å
• α: 90°
• β: 90.84 ± 0.003°
• γ: 90°
• Cell volume: 5672.3 ± 0.5 ų
• Cell temperature: 133 ± 2 K
• Ambient diffraction temperature: 133 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.1802
• Residual factor for significantly intense reflections: 0.0619
• Weighted residual factors for significantly intense reflections: 0.1011
• Weighted residual factors for all reflections included in the refinement: 0.1332
• Goodness-of-fit parameter for all reflections included in the refinement: 0.97
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No