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Information card for entry 7029318
Preview
Coordinates | 7029318.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C18 H29 B10 Ir N2 O2 S2 |
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Calculated formula | C18 H29 B10 Ir N2 O2 S2 |
Title of publication | Radical coupling for directed C-C/C-S bond formation in the reaction of Cp*IrS2C2B10H10 with 1-azido-3-nitrobenzene. |
Authors of publication | Zhong, Wei; Jiang, Qibai; Zhang, Qian; Shang, Yi; Yan, Hong; Bregadze, Vladimir |
Journal of publication | Dalton transactions (Cambridge, England : 2003) |
Year of publication | 2014 |
Journal volume | 43 |
Journal issue | 13 |
Pages of publication | 4962 - 4968 |
a | 11.7159 ± 0.0013 Å |
b | 14.4682 ± 0.0016 Å |
c | 17.9172 ± 0.0019 Å |
α | 69.271 ± 0.002° |
β | 72.654 ± 0.002° |
γ | 72.994 ± 0.002° |
Cell volume | 2651.2 ± 0.5 Å3 |
Cell temperature | 296 ± 2 K |
Ambient diffraction temperature | 296 ± 2 K |
Number of distinct elements | 7 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0428 |
Residual factor for significantly intense reflections | 0.0344 |
Weighted residual factors for significantly intense reflections | 0.0871 |
Weighted residual factors for all reflections included in the refinement | 0.0909 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.063 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
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