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Information card for entry 7029423
Preview
Coordinates | 7029423.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C15 H20 Cl2 N2 O2 Pd |
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Calculated formula | C15 H20 Cl2 N2 O2 Pd |
SMILES | [Pd]12(c3c(ccc(c3[C@H](C)[N]1(C)C)Cl)Cl)[NH]1[C@H](C(=O)O2)CCC1 |
Title of publication | Development of a novel chiral palladacycle and its application in asymmetric hydrophosphination reaction. |
Authors of publication | Yap, Jeanette See Leng; Li, Bin Bin; Wong, Jonathan; Li, Yongxin; Pullarkat, Sumod A.; Leung, Pak-Hing |
Journal of publication | Dalton transactions (Cambridge, England : 2003) |
Year of publication | 2014 |
Journal volume | 43 |
Journal issue | 15 |
Pages of publication | 5777 - 5784 |
a | 6.7161 ± 0.0002 Å |
b | 8.8109 ± 0.0003 Å |
c | 14.4813 ± 0.0005 Å |
α | 90° |
β | 102.699 ± 0.001° |
γ | 90° |
Cell volume | 835.97 ± 0.05 Å3 |
Cell temperature | 103 ± 2 K |
Ambient diffraction temperature | 103 ± 2 K |
Number of distinct elements | 6 |
Space group number | 4 |
Hermann-Mauguin space group symbol | P 1 21 1 |
Hall space group symbol | P 2yb |
Residual factor for all reflections | 0.0187 |
Residual factor for significantly intense reflections | 0.0181 |
Weighted residual factors for significantly intense reflections | 0.0434 |
Weighted residual factors for all reflections included in the refinement | 0.0479 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.106 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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