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Information card for entry 7029434
Preview
Coordinates | 7029434.cif |
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Original paper (by DOI) | HTML |
Formula | C35 H35 Cl2 N3 O4 P Re |
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Calculated formula | C35 H35 Cl2 N3 O4 P Re |
SMILES | [Re]1([n]2[nH]c3c(c2C(=O)O1)cccc3)(=Nc1ccc(cc1)C)([P](c1ccccc1)(c1ccccc1)c1ccccc1)(Cl)Cl.OC.OC |
Title of publication | New p-tolylimido rhenium(v) complexes with carboxylate-based ligands: synthesis, structures and their catalytic potential in oxidations with peroxides. |
Authors of publication | Gryca, I.; Machura, B.; Małecki, J G; Shul'pina, Lidia S.; Pombeiro, Armando J. L.; Shul'pin, Georgiy B. |
Journal of publication | Dalton transactions (Cambridge, England : 2003) |
Year of publication | 2014 |
Journal volume | 43 |
Journal issue | 15 |
Pages of publication | 5759 - 5776 |
a | 8.2043 ± 0.0016 Å |
b | 11.196 ± 0.002 Å |
c | 18.785 ± 0.004 Å |
α | 84.91 ± 0.03° |
β | 84.9 ± 0.03° |
γ | 85.4 ± 0.03° |
Cell volume | 1707.3 ± 0.6 Å3 |
Cell temperature | 293 ± 2 K |
Ambient diffraction temperature | 293 ± 2 K |
Number of distinct elements | 7 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0374 |
Residual factor for significantly intense reflections | 0.0305 |
Weighted residual factors for significantly intense reflections | 0.0626 |
Weighted residual factors for all reflections included in the refinement | 0.065 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.027 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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The link is: https://www.crystallography.net/7029434.html
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