Information card for entry 7029482

Structure parameters

• Formula: C59 H84 Al Ge N4 O2
• Calculated formula: C59 H84 Al Ge N4 O2
• Title of publication: Mechanistic studies of CO2 reduction to methanol mediated by an N-heterocyclic germylene hydride.
• Authors of publication: Tan, Gengwen; Wang, Wenyuan; Blom, Burgert; Driess, Matthias
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2014
• Journal volume: 43
• Journal issue: 16
• Pages of publication: 6006 - 6011
• a: 24.8625 ± 0.0003 Å
• b: 15.1844 ± 0.0002 Å
• c: 14.7693 ± 0.0002 Å
• α: 90°
• β: 94.271 ± 0.001°
• γ: 90°
• Cell volume: 5560.25 ± 0.12 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 6
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0474
• Residual factor for significantly intense reflections: 0.0437
• Weighted residual factors for significantly intense reflections: 0.1225
• Weighted residual factors for all reflections included in the refinement: 0.1291
• Goodness-of-fit parameter for all reflections included in the refinement: 1.022
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No