Information card for entry 7029563

Structure parameters

• Formula: C15 H39 Ge2 N O3 Si3
• Calculated formula: C15 H39.5 Ge2 N O3 Si3
• Title of publication: New oligogermane with a five coordinate germanium atom: the preparation of 1-germylgermatrane.
• Authors of publication: Zaitsev, Kirill V.; Churakov, Andrei V.; Poleshchuk, Oleg Kh; Oprunenko, Yuri F.; Zaitseva, Galina S.; Karlov, Sergey S.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2014
• Journal volume: 43
• Journal issue: 18
• Pages of publication: 6605 - 6609
• a: 11.3567 ± 0.0016 Å
• b: 27.748 ± 0.004 Å
• c: 16.127 ± 0.002 Å
• α: 90°
• β: 102.683 ± 0.002°
• γ: 90°
• Cell volume: 4958 ± 1.2 ų
• Cell temperature: 130 ± 2 K
• Ambient diffraction temperature: 130 ± 2 K
• Number of distinct elements: 6
• Space group number: 11
• Hermann-Mauguin space group symbol: P 1 21/m 1
• Hall space group symbol: -P 2yb
• Residual factor for all reflections: 0.1066
• Residual factor for significantly intense reflections: 0.0592
• Weighted residual factors for significantly intense reflections: 0.1248
• Weighted residual factors for all reflections included in the refinement: 0.1391
• Goodness-of-fit parameter for all reflections included in the refinement: 1.055
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No