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Information card for entry 7029585
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Coordinates | 7029585.cif |
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Original paper (by DOI) | HTML |
Formula | C88 H44 B2 F48 N10 O4 Rh2 |
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Calculated formula | C88 H44 B2 F48 N10 O4 Rh2 |
Title of publication | Bi- and tri-metallic Rh and Ir complexes containing click derived bis- and tris-(pyrazolyl-1,2,3-triazolyl) N-N' donor ligands and their application as catalysts for the dihydroalkoxylation of alkynes. |
Authors of publication | Vuong, Khuong Q.; Wong, Chin M.; Bhadbhade, Mohan; Messerle, Barbara A. |
Journal of publication | Dalton transactions (Cambridge, England : 2003) |
Year of publication | 2014 |
Journal volume | 43 |
Journal issue | 20 |
Pages of publication | 7540 - 7553 |
a | 13.054 ± 0.003 Å |
b | 13.837 ± 0.003 Å |
c | 15.174 ± 0.003 Å |
α | 69.18 ± 0.03° |
β | 73.8 ± 0.03° |
γ | 64.55 ± 0.03° |
Cell volume | 2287.2 ± 1.1 Å3 |
Cell temperature | 100 ± 2 K |
Ambient diffraction temperature | 100 ± 2 K |
Number of distinct elements | 7 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0385 |
Residual factor for significantly intense reflections | 0.0365 |
Weighted residual factors for significantly intense reflections | 0.0923 |
Weighted residual factors for all reflections included in the refinement | 0.0936 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.049 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | Synchrotron |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
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The link is: https://www.crystallography.net/7029585.html
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