Information card for entry 7029639

Structure parameters

• Formula: C65 H93 Cl O13 P2 Ru Si8
• Calculated formula: C65 H93 Cl O13 P2 Ru Si8
• Title of publication: The first ruthenium-silsesquioxyl complexes - synthesis, structure and mechanistic implications in silylative coupling.
• Authors of publication: Zak, Patrycja; Kubicki, Maciej; Marciniec, Bogdan; Rogalski, Szymon; Pietraszuk, Cezary; Frąckowiak, Dawid
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2014
• Journal volume: 43
• Journal issue: 21
• Pages of publication: 7911 - 7916
• a: 13.491 ± 0.0003 Å
• b: 14.8072 ± 0.0003 Å
• c: 19.0764 ± 0.0004 Å
• α: 89.338 ± 0.002°
• β: 81.06 ± 0.002°
• γ: 77.729 ± 0.002°
• Cell volume: 3677.57 ± 0.14 ų
• Cell temperature: 100 ± 1 K
• Ambient diffraction temperature: 100 ± 1 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0417
• Residual factor for significantly intense reflections: 0.0307
• Weighted residual factors for significantly intense reflections: 0.0706
• Weighted residual factors for all reflections included in the refinement: 0.0754
• Goodness-of-fit parameter for all reflections included in the refinement: 1.038
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No