Information card for entry 7029679

Structure parameters

• Formula: C40 H75 B N O2 P3 Rh
• Calculated formula: C40 H75 B N O2 P3 Rh
• Title of publication: Versatile reactivity of a rhodium(i) boryl complex towards ketones and imines.
• Authors of publication: Kalläne, Sabrina I; Braun, Thomas; Braun, Beatrice; Mebs, Stefan
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2014
• Journal volume: 43
• Journal issue: 18
• Pages of publication: 6786 - 6801
• a: 42.3611 ± 0.0015 Å
• b: 10.5311 ± 0.0002 Å
• c: 23.6156 ± 0.0008 Å
• α: 90°
• β: 120.338 ± 0.003°
• γ: 90°
• Cell volume: 9092.5 ± 0.6 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 7
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0692
• Residual factor for significantly intense reflections: 0.0567
• Weighted residual factors for significantly intense reflections: 0.1529
• Weighted residual factors for all reflections included in the refinement: 0.163
• Goodness-of-fit parameter for all reflections included in the refinement: 1.059
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No