Information card for entry 7029730

Structure parameters

• Formula: C44 H65 Lu N P Si2
• Calculated formula: C44 H65 Lu N P Si2
• Title of publication: Tetrahydropentalenyl-phosphazene constrained geometry complexes of rare-earth metal alkyls.
• Authors of publication: Hangaly, Noa K; Petrov, Alexander R; Elfferding, Michael; Harms, Klaus; Sundermeyer, Jörg
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2014
• Journal volume: 43
• Journal issue: 19
• Pages of publication: 7109 - 7120
• a: 19.2484 ± 0.0007 Å
• b: 20.4463 ± 0.0006 Å
• c: 23.1053 ± 0.0008 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 9093.3 ± 0.5 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 6
• Space group number: 61
• Hermann-Mauguin space group symbol: P b c a
• Hall space group symbol: -P 2ac 2ab
• Residual factor for all reflections: 0.0656
• Residual factor for significantly intense reflections: 0.0309
• Weighted residual factors for significantly intense reflections: 0.0405
• Weighted residual factors for all reflections included in the refinement: 0.0452
• Goodness-of-fit parameter for all reflections included in the refinement: 0.866
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No