Information card for entry 7029853

Structure parameters

• Formula: C22.5 H34 B2 Br2 N8 Sn
• Calculated formula: C22.5 H34 B2 Br2 N8 Sn
• Title of publication: Overcoming NHCs neutrality: installing tetracarbenes on group 13 and 14 metals.
• Authors of publication: Cramer, S. Alan; Sturgill, Forrest L.; Chandrachud, Preeti P.; Jenkins, David M.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2014
• Journal volume: 43
• Journal issue: 21
• Pages of publication: 7687 - 7690
• a: 12.9886 ± 0.0008 Å
• b: 13.3288 ± 0.0008 Å
• c: 14.4878 ± 0.0009 Å
• α: 117.22 ± 0.001°
• β: 94.9 ± 0.001°
• γ: 103.066 ± 0.001°
• Cell volume: 2120.4 ± 0.2 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0424
• Residual factor for significantly intense reflections: 0.032
• Weighted residual factors for significantly intense reflections: 0.0822
• Weighted residual factors for all reflections included in the refinement: 0.0911
• Goodness-of-fit parameter for all reflections included in the refinement: 1.006
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No