Information card for entry 7029876

Structure parameters

• Formula: C32 H56 Mo N2 P2 Si3
• Calculated formula: C32 H56 Mo N2 P2 Si3
• Title of publication: Multiple coupling of silanes with imido complexes of Mo.
• Authors of publication: Khalimon, Andrey Y.; McLeod, Nicolas A.; Ignatov, Stanislav K.; Okhapkin, Andrey I.; Kuzmina, Lyudmila G.; Howard, Judith A. K.; Nikonov, Georgii I.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2014
• Journal volume: 43
• Journal issue: 22
• Pages of publication: 8446 - 8453
• a: 10.893 ± 0.003 Å
• b: 22.133 ± 0.007 Å
• c: 15.524 ± 0.005 Å
• α: 90°
• β: 100.687 ± 0.014°
• γ: 90°
• Cell volume: 3678 ± 2 ų
• Cell temperature: 123 ± 2 K
• Ambient diffraction temperature: 123.15 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.3144
• Residual factor for significantly intense reflections: 0.096
• Weighted residual factors for significantly intense reflections: 0.1983
• Weighted residual factors for all reflections included in the refinement: 0.2576
• Goodness-of-fit parameter for all reflections included in the refinement: 0.733
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No