Information card for entry 7030089

Structure parameters

• Formula: C63 H46 N6 O48 Pb10
• Calculated formula: C63 H42 N6 O48 Pb10
• Title of publication: An unusual chiral 3D inorganic connectivity featuring a {Pb18} wheel: rapid and highly selective and sensitive sensing of Co(ii).
• Authors of publication: Han, Yun-Hu; Tian, Chong-Bin; Du, Shao-Wu
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2014
• Journal volume: 43
• Journal issue: 30
• Pages of publication: 11461 - 11464
• a: 15.729 ± 0.002 Å
• b: 15.729 ± 0.002 Å
• c: 30.451 ± 0.006 Å
• α: 90°
• β: 90°
• γ: 120°
• Cell volume: 6524.3 ± 1.7 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 5
• Space group number: 152
• Hermann-Mauguin space group symbol: P 31 2 1
• Hall space group symbol: P 31 2"
• Residual factor for all reflections: 0.0693
• Residual factor for significantly intense reflections: 0.0679
• Weighted residual factors for significantly intense reflections: 0.1777
• Weighted residual factors for all reflections included in the refinement: 0.1789
• Goodness-of-fit parameter for all reflections included in the refinement: 0.981
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No