Information card for entry 7030115

Structure parameters

• Formula: C32 H92 N20 S18 Sb8 Sm4
• Calculated formula: C32 H92 N20 S18 Sb8 Sm4
• Title of publication: Novel lanthanoid thioantimonates: the first coexistence of different types of thioantimonate anions in the same framework.
• Authors of publication: Zhou, Jian; Hu, Feilong; An, Litao; Liu, Xing; Meng, Chang-yu
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2012
• Journal volume: 41
• Journal issue: 38
• Pages of publication: 11760 - 11764
• a: 9.6338 ± 0.0019 Å
• b: 14.685 ± 0.003 Å
• c: 16.265 ± 0.003 Å
• α: 116.67 ± 0.03°
• β: 96.56 ± 0.03°
• γ: 98.88 ± 0.03°
• Cell volume: 1987.2 ± 1 ų
• Cell temperature: 296 ± 2 K
• Ambient diffraction temperature: 296 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0558
• Residual factor for significantly intense reflections: 0.0521
• Weighted residual factors for significantly intense reflections: 0.1427
• Weighted residual factors for all reflections included in the refinement: 0.1474
• Goodness-of-fit parameter for all reflections included in the refinement: 1.03
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No