Information card for entry 7030349

Structure parameters

• Chemical name: Poly[bis-[μ~4~-[1,3-bis(pyridazin-4-yl)adamantane-κ^4^N1:N2:N3:N4)]]- tetrakis-[μ~2~-(5-hydroxy-1,3-benzenedicarboxylato)]-di(μ~2~-hydroxido)- diaquapentacopper(II)] hexahydrate
• Formula: C68 H74 Cu5 N8 O30
• Calculated formula: C68 H74 Cu5 N8 O30
• Title of publication: Mixed-ligand hydroxocopper(ii)/pyridazine clusters embedded into 3D framework lattices.
• Authors of publication: Degtyarenko, Anna S.; Handke, Marcel; Krämer, Karl W; Liu, Shi-Xia; Decurtins, Silvio; Rusanov, Eduard B.; Thompson, Laurence K.; Krautscheid, Harald; Domasevitch, Konstantin V.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2014
• Journal volume: 43
• Journal issue: 22
• Pages of publication: 8530 - 8542
• a: 10.0552 ± 0.0005 Å
• b: 18.784 ± 0.0008 Å
• c: 19.1757 ± 0.0009 Å
• α: 90°
• β: 104.829 ± 0.002°
• γ: 90°
• Cell volume: 3501.2 ± 0.3 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0941
• Residual factor for significantly intense reflections: 0.0471
• Weighted residual factors for significantly intense reflections: 0.0887
• Weighted residual factors for all reflections included in the refinement: 0.1045
• Goodness-of-fit parameter for all reflections included in the refinement: 1.01
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No