Information card for entry 7030356

Structure parameters

• Formula: C37 H46 Cl Fe N6 O6
• Calculated formula: C37 H46 Cl Fe N6 O6
• Title of publication: N-2-Hydroxybenzaldehyde acylhydrazone-Fe(iii) complex: synthesis, crystal structure and its efficient and selective N-methylation.
• Authors of publication: Li, Zhiyou; Wu, Lamei; Zhang, Tao; Huang, Zhengxi; Qiu, Guofu; Zhou, Zhongqiang; Jin, Longfei
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2014
• Journal volume: 43
• Journal issue: 20
• Pages of publication: 7554 - 7560
• a: 12.311 ± 0.004 Å
• b: 13.132 ± 0.004 Å
• c: 14.299 ± 0.005 Å
• α: 99.409 ± 0.004°
• β: 108.611 ± 0.004°
• γ: 98.761 ± 0.005°
• Cell volume: 2109 ± 1.2 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1335
• Residual factor for significantly intense reflections: 0.0888
• Weighted residual factors for significantly intense reflections: 0.2001
• Weighted residual factors for all reflections included in the refinement: 0.2299
• Goodness-of-fit parameter for all reflections included in the refinement: 0.986
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No