Information card for entry 7030735

Structure parameters

• Formula: C24 H81 Co3 N6 Na2 O56 P W10
• Calculated formula: C24 H32 Co3 N6 Na O58.5 P W10
• Title of publication: Grafting ligands to direct the self-assembly of Co/Ni2+ substituted polyoxometalate clusters
• Authors of publication: Ritchie, Chris; Boyd, Thomas; Long, De-Liang; Ditzel, Evert; Cronin, Leroy
• Journal of publication: Dalton Transactions
• Year of publication: 2009
• Journal issue: 9
• Pages of publication: 1587 - 1592
• a: 19.8809 ± 0.0006 Å
• b: 15.1911 ± 0.0004 Å
• c: 25.0011 ± 0.0007 Å
• α: 90°
• β: 106.846 ± 0.002°
• γ: 90°
• Cell volume: 7226.6 ± 0.4 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 8
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0557
• Residual factor for significantly intense reflections: 0.0357
• Weighted residual factors for significantly intense reflections: 0.0718
• Weighted residual factors for all reflections included in the refinement: 0.0793
• Goodness-of-fit parameter for all reflections included in the refinement: 1.027
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Duplicate of: 7000577
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No