Information card for entry 7030739

Structure parameters

• Formula: C16 H33 N3 O Si Ti
• Calculated formula: C16 H33 N3 O Si Ti
• Title of publication: Transformation of hydroxylamide into hydrazide units in the coordination spheres of group 4 metals
• Authors of publication: Willner, Alexander; Neumann, Beate; Stammler, Hans-Georg; Mitzel, Norbert W.
• Journal of publication: Dalton Transactions
• Year of publication: 2009
• Journal issue: 32
• Pages of publication: 6280 - 6282
• a: 14.9808 ± 0.0007 Å
• b: 10.0118 ± 0.0004 Å
• c: 26.2621 ± 0.0009 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 3938.9 ± 0.3 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 64
• Hermann-Mauguin space group symbol: C m c a
• Hall space group symbol: -C 2ac 2
• Residual factor for all reflections: 0.0681
• Residual factor for significantly intense reflections: 0.0429
• Weighted residual factors for significantly intense reflections: 0.1058
• Weighted residual factors for all reflections included in the refinement: 0.1157
• Goodness-of-fit parameter for all reflections included in the refinement: 1.047
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Duplicate of: 7001796
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No