Information card for entry 7030938

Structure parameters

• Formula: C112 H112 N6 O2 P4 Sm2
• Calculated formula: C112 H112 N6 O2 P4 Sm2
• Title of publication: Differences in the cyclometalation reactivity of bisphosphinimine-supported organo-rare earth complexes.
• Authors of publication: Zamora, Matthew T.; Johnson, Kevin R. D.; Hänninen, Mikko M; Hayes, Paul G.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2014
• Journal volume: 43
• Journal issue: 28
• Pages of publication: 10739 - 10750
• a: 15.9755 ± 0.0013 Å
• b: 17.8486 ± 0.0015 Å
• c: 17.3855 ± 0.0014 Å
• α: 90°
• β: 109.203 ± 0.001°
• γ: 90°
• Cell volume: 4681.5 ± 0.7 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173.15 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0244
• Residual factor for significantly intense reflections: 0.0199
• Weighted residual factors for significantly intense reflections: 0.0473
• Weighted residual factors for all reflections included in the refinement: 0.0499
• Goodness-of-fit parameter for all reflections included in the refinement: 1.033
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No