Crystallography Open Database

Information card for entry 7031083

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Coordinates	7031083.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C25 H28 N O6 V
Calculated formula	C25 H28 N O6 V
Title of publication	Biphenyl derived Schiff-base vanadium(V) complexes with pendant OH-groups‒structure, characterization and hydrogen peroxide mediated sulfide oxygenation.
Authors of publication	Plitt, Patrick; Pritzkow, Hans; Kramer, Roland
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2004
Journal issue	15
Pages of publication	2314 - 2320
a	12.4475 ± 0.0006 Å
b	29.3169 ± 0.0014 Å
c	6.9933 ± 0.0003 Å
α	90°
β	113.764 ± 0.001°
γ	90°
Cell volume	2335.63 ± 0.19 Å³
Cell temperature	103 ± 2 K
Ambient diffraction temperature	103 ± 2 K
Number of distinct elements	5
Space group number	9
Hermann-Mauguin space group symbol	C 1 c 1
Hall space group symbol	C -2yc
Residual factor for all reflections	0.0408
Residual factor for significantly intense reflections	0.0347
Weighted residual factors for significantly intense reflections	0.0804
Weighted residual factors for all reflections included in the refinement	0.0845
Goodness-of-fit parameter for all reflections included in the refinement	1.03
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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