Information card for entry 7031148

Structure parameters

• Formula: C21 H36 Cl3 O P Pd
• Calculated formula: C21 H36 Cl3 O P Pd
• Title of publication: Orthopalladated phosphinite complexes as high-activity catalysts for the Suzuki reactionBased on the presentation given at Dalton Discussion No. 6, 9?11th September 2003, University of York, UK.
• Authors of publication: Bedford, Robin B.; Hazelwood (n�e Welch), Samantha L.; Horton, Peter N.; Hursthouse, Michael B.
• Journal of publication: Dalton Transactions
• Year of publication: 2003
• Journal issue: 21
• Pages of publication: 4164
• a: 10.6317 ± 0.0001 Å
• b: 22.1407 ± 0.0003 Å
• c: 11.3297 ± 0.0002 Å
• α: 90°
• β: 112.61°
• γ: 90°
• Cell volume: 2461.96 ± 0.06 ų
• Cell temperature: 120 ± 2 K
• Ambient diffraction temperature: 120 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0336
• Residual factor for significantly intense reflections: 0.0283
• Weighted residual factors for significantly intense reflections: 0.069
• Weighted residual factors for all reflections included in the refinement: 0.0715
• Goodness-of-fit parameter for all reflections included in the refinement: 1.055
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No