Crystallography Open Database

Information card for entry 7031277

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Coordinates	7031277.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C22 H31 N Si
Calculated formula	C22 H31 N Si
Title of publication	Hydrometallation of amino-trialkynylsilanes - intramolecular M-N interactions (M = Al, Ga) and potential activation of Si-N bonds.
Authors of publication	Uhl, Werner; Bohnemann, Jörg; Kappelt, Benedikt; Hepp, Alexander; Layh, Marcus
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2014
Journal volume	43
Journal issue	38
Pages of publication	14386 - 14398
a	10.0207 ± 0.0002 Å
b	13.4721 ± 0.0002 Å
c	16.8224 ± 0.0003 Å
α	90°
β	90°
γ	90°
Cell volume	2271.02 ± 0.07 Å³
Cell temperature	153 ± 2 K
Ambient diffraction temperature	153 ± 2 K
Number of distinct elements	4
Space group number	19
Hermann-Mauguin space group symbol	P 21 21 21
Hall space group symbol	P 2ac 2ab
Residual factor for all reflections	0.0447
Residual factor for significantly intense reflections	0.039
Weighted residual factors for significantly intense reflections	0.0911
Weighted residual factors for all reflections included in the refinement	0.0944
Goodness-of-fit parameter for all reflections included in the refinement	1.059
Diffraction radiation wavelength	1.54178 Å
Diffraction radiation type	CuKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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