Information card for entry 7031340

Structure parameters

• Formula: C105 H157 Lu3 N6 O2 Si
• Calculated formula: C105 H157 Lu3 N6 O2 Si
• Title of publication: Trinuclear alkyl hydrido rare-earth complexes supported by amidopyridinato ligands: synthesis, structures, C-Si bond activation and catalytic activity in ethylene polymerization.
• Authors of publication: Lyubov, Dmitry M.; Cherkasov, Anton V.; Fukin, Georgy K.; Ketkov, Sergey Yu; Shavyrin, Andrey S.; Trifonov, Alexander A.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2014
• Journal volume: 43
• Journal issue: 38
• Pages of publication: 14450 - 14460
• a: 16.3929 ± 0.0014 Å
• b: 17.2417 ± 0.0014 Å
• c: 20.1103 ± 0.0016 Å
• α: 88.307 ± 0.006°
• β: 74.884 ± 0.006°
• γ: 83.034 ± 0.006°
• Cell volume: 5446.8 ± 0.8 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1316
• Residual factor for significantly intense reflections: 0.0538
• Weighted residual factors for significantly intense reflections: 0.0742
• Weighted residual factors for all reflections included in the refinement: 0.0864
• Goodness-of-fit parameter for all reflections included in the refinement: 0.769
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No