Information card for entry 7031597

Structure parameters

• Formula: C4 H12 N8 Ni
• Calculated formula: C4 H12 N8 Ni
• Title of publication: Synthesis, crystal structure and magnetic properties of two alternating double μ1,1 and μ1,3 azido bridged Cu(ii) and Ni(ii) chains.
• Authors of publication: Bhowmik, Pallab; Biswas, Saptarshi; Chattopadhyay, Shouvik; Diaz, Carmen; Gómez-García, Carlos J; Ghosh, Ashutosh
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2014
• Journal volume: 43
• Journal issue: 32
• Pages of publication: 12414 - 12421
• a: 6.8792 ± 0.0018 Å
• b: 7.669 ± 0.002 Å
• c: 10.216 ± 0.003 Å
• α: 80.328 ± 0.003°
• β: 88.967 ± 0.003°
• γ: 64.213 ± 0.003°
• Cell volume: 477.5 ± 0.2 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 4
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0563
• Residual factor for significantly intense reflections: 0.0435
• Weighted residual factors for significantly intense reflections: 0.1122
• Weighted residual factors for all reflections included in the refinement: 0.1218
• Goodness-of-fit parameter for all reflections included in the refinement: 1.023
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No