Information card for entry 7031671

Structure parameters

• Formula: C13 H14 B N9 O Pb S8
• Calculated formula: C13 H14 B N9 O Pb S8
• Title of publication: Hemi- and holo-directed lead(II) complexes in a soft ligand environment.
• Authors of publication: Imran, Muhammad; Mix, Andreas; Neumann, Beate; Stammler, Hans-Georg; Monkowius, Uwe; Gründlinger, Petra; Mitzel, Norbert W.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2015
• Journal volume: 44
• Journal issue: 3
• Pages of publication: 924 - 937
• a: 10.1258 ± 0.0009 Å
• b: 11.5049 ± 0.0011 Å
• c: 12.799 ± 0.0019 Å
• α: 111.827 ± 0.006°
• β: 108.21 ± 0.006°
• γ: 95.805 ± 0.005°
• Cell volume: 1274.3 ± 0.3 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0153
• Residual factor for significantly intense reflections: 0.015
• Weighted residual factors for significantly intense reflections: 0.0354
• Weighted residual factors for all reflections included in the refinement: 0.0356
• Goodness-of-fit parameter for all reflections included in the refinement: 1.047
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No