Information card for entry 7031741

Structure parameters

• Formula: C46.5 H57.5 B2 N12 O U
• Calculated formula: C46.5 H54 B2 N12 O U
• Title of publication: Isolation of a uranium(iii) benzophenone ketyl radical that displays redox-active ligand behaviour.
• Authors of publication: Matson, Ellen M.; Kiernicki, John J.; Anderson, Nickolas H.; Fanwick, Phillip E.; Bart, Suzanne C.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2014
• Journal volume: 43
• Journal issue: 48
• Pages of publication: 17885 - 17888
• a: 11.0395 ± 0.0008 Å
• b: 13.5231 ± 0.0009 Å
• c: 17.6638 ± 0.0018 Å
• α: 72.59 ± 0.005°
• β: 86.21 ± 0.005°
• γ: 67.426 ± 0.004°
• Cell volume: 2319.9 ± 0.3 ų
• Cell temperature: 150 ± 0.02 K
• Ambient diffraction temperature: 150 ± 0.02 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.069
• Residual factor for significantly intense reflections: 0.068
• Weighted residual factors for significantly intense reflections: 0.179
• Weighted residual factors for all reflections included in the refinement: 0.18
• Goodness-of-fit parameter for all reflections included in the refinement: 1.086
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CU-Kα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No