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Information card for entry 7031772
Preview
Coordinates | 7031772.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C103 H134.5 N3.5 O16 W2 |
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Calculated formula | C103 H132.834 N3.5 O16 W2 |
Title of publication | Ethyleneglycol tungsten complexes of calix[6 and 8]arenes: synthesis, characterization and ROP of ε-caprolactone. |
Authors of publication | Li, Yuanzhuo; Zhao, Ke-Qing; Feng, Chun; Elsegood, Mark R. J.; Prior, Timothy J.; Sun, Xinsen; Redshaw, Carl |
Journal of publication | Dalton transactions (Cambridge, England : 2003) |
Year of publication | 2014 |
Journal volume | 43 |
Journal issue | 36 |
Pages of publication | 13612 - 13619 |
a | 14.8901 ± 0.0011 Å |
b | 17.5516 ± 0.0013 Å |
c | 22.0164 ± 0.0016 Å |
α | 112.022 ± 0.0009° |
β | 105.391 ± 0.001° |
γ | 93.0486 ± 0.001° |
Cell volume | 5067.2 ± 0.6 Å3 |
Cell temperature | 150 ± 2 K |
Ambient diffraction temperature | 150 ± 2 K |
Number of distinct elements | 5 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.1172 |
Residual factor for significantly intense reflections | 0.0763 |
Weighted residual factors for significantly intense reflections | 0.1588 |
Weighted residual factors for all reflections included in the refinement | 0.175 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.113 |
Diffraction radiation wavelength | 0.6884 Å |
Diffraction radiation type | synchrotron |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
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