Information card for entry 7031867

Structure parameters

• Chemical name: dimethyl-trans-bis-trimethylphosphine-nickle(ii)
• Formula: C8 H24 Ni P2
• Calculated formula: C8 H24 Ni P2
• Title of publication: Synthesis and structures of mononuclear 3,4-bis(trifluoromethyl)pyrrolyl complexes of Rh(i) and Ni(ii).
• Authors of publication: Rivers, Joseph H.; Jones, Richard A.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2014
• Journal volume: 43
• Journal issue: 43
• Pages of publication: 16275 - 16282
• a: 5.41 ± 0.005 Å
• b: 15.773 ± 0.003 Å
• c: 8.449 ± 0.005 Å
• α: 90°
• β: 118.57 ± 0.04°
• γ: 90°
• Cell volume: 633.2 ± 0.7 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 4
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.1275
• Residual factor for significantly intense reflections: 0.1035
• Weighted residual factors for significantly intense reflections: 0.1846
• Weighted residual factors for all reflections included in the refinement: 0.1965
• Goodness-of-fit parameter for all reflections included in the refinement: 1.257
• Diffraction radiation wavelength: 0.71069 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No