Information card for entry 7031977

Structure parameters

• Formula: C17 H23 Cl3 F6 N O Ru Sb
• Calculated formula: C17 H23 Cl3 F6 N O Ru Sb
• SMILES: [Ru]123456(Cl)([OH]Cc7[n]1cccc7)[c]1([cH]6[cH]5[c]4([cH]3[cH]21)C)C(C)C.C(Cl)Cl.[Sb](F)(F)(F)(F)(F)[F-]
• Title of publication: Hydroxymethylpyridine containing half-sandwich complexes of Rh(iii), Ir(iii) or Ru(ii).
• Authors of publication: Carmona, Daniel; Lamata, Pilar; Sánchez, Antonio; Pardo, Pilar; Rodríguez, Ricardo; Ramírez, Paola; Lahoz, Fernando J.; García-Orduña, Pilar; Oro, Luis A.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2014
• Journal volume: 43
• Journal issue: 41
• Pages of publication: 15546 - 15559
• a: 11.041 ± 0.001 Å
• b: 11.4271 ± 0.0011 Å
• c: 12.276 ± 0.001 Å
• α: 62.566 ± 0.001°
• β: 64.008 ± 0.001°
• γ: 61.41 ± 0.001°
• Cell volume: 1158.95 ± 0.18 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0774
• Residual factor for significantly intense reflections: 0.0532
• Weighted residual factors for significantly intense reflections: 0.121
• Weighted residual factors for all reflections included in the refinement: 0.1355
• Goodness-of-fit parameter for all reflections included in the refinement: 0.844
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No