Crystallography Open Database

Information card for entry 7032019

7032018 << 7032019 >> 7032020

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Coordinates	7032019.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C52 H74 Co4 N32 O11
Calculated formula	C52 H60 Co4 N32 O11
Title of publication	Unprecedented dinuclear Robson type macrocyclic complexes having two +iii metal ions in two compartments and the role of the diimino moiety on the stability of metal ion oxidation states.
Authors of publication	Mandal, Leena; Mohanta, Sasankasekhar
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2014
Journal volume	43
Journal issue	42
Pages of publication	15737 - 15751
a	27.05 ± 0.02 Å
b	13.151 ± 0.011 Å
c	23.69 ± 0.03 Å
α	90°
β	124.351 ± 0.009°
γ	90°
Cell volume	6958 ± 12 Å³
Cell temperature	296 ± 2 K
Ambient diffraction temperature	296 ± 2 K
Number of distinct elements	5
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.101
Residual factor for significantly intense reflections	0.0583
Weighted residual factors for significantly intense reflections	0.1608
Weighted residual factors for all reflections included in the refinement	0.1864
Goodness-of-fit parameter for all reflections included in the refinement	1.046
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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