Crystallography Open Database

Information card for entry 7032021

7032020 << 7032021 >> 7032022

Preview

Coordinates	7032021.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C56 H76 Co4 N26 O8
Calculated formula	C56 H68 Co4 N26 O7
Title of publication	Unprecedented dinuclear Robson type macrocyclic complexes having two +iii metal ions in two compartments and the role of the diimino moiety on the stability of metal ion oxidation states.
Authors of publication	Mandal, Leena; Mohanta, Sasankasekhar
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2014
Journal volume	43
Journal issue	42
Pages of publication	15737 - 15751
a	13.058 ± 0.006 Å
b	20.926 ± 0.01 Å
c	25.25 ± 0.012 Å
α	90°
β	98.881 ± 0.006°
γ	90°
Cell volume	6817 ± 6 Å³
Cell temperature	296 ± 2 K
Ambient diffraction temperature	296 ± 2 K
Number of distinct elements	5
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/n 1
Hall space group symbol	-P 2yn
Residual factor for all reflections	0.1246
Residual factor for significantly intense reflections	0.0837
Weighted residual factors for significantly intense reflections	0.1968
Weighted residual factors for all reflections included in the refinement	0.2162
Goodness-of-fit parameter for all reflections included in the refinement	1.029
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/7032021.html