Information card for entry 7032073

Structure parameters

• Formula: C94 H110 B4 F16 Mo4 N10 O8 P4
• Calculated formula: C94 H110 B4 F16 Mo4 N10 O8 P4
• Title of publication: Loop shaped dicarboxylate-bridged dimolybdenum(ii) bisphosphine compounds - a rational synthesis.
• Authors of publication: Höhne, Dominik; Herdtweck, Eberhardt; Pöthig, Alexander; Kühn, Fritz E
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2014
• Journal volume: 43
• Journal issue: 41
• Pages of publication: 15367 - 15374
• a: 12.4049 ± 0.0005 Å
• b: 18.0187 ± 0.0007 Å
• c: 24.6268 ± 0.001 Å
• α: 74.092 ± 0.002°
• β: 88.172 ± 0.002°
• γ: 81.785 ± 0.002°
• Cell volume: 5239.3 ± 0.4 ų
• Cell temperature: 123 K
• Ambient diffraction temperature: 123 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0717
• Residual factor for significantly intense reflections: 0.0533
• Weighted residual factors for significantly intense reflections: 0.1247
• Weighted residual factors for all reflections included in the refinement: 0.1408
• Goodness-of-fit parameter for all reflections included in the refinement: 1.066
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No