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Information card for entry 7032146
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Coordinates | 7032146.cif |
---|---|
Original paper (by DOI) | HTML |
Chemical name | (NEt4)2[WO{S2C6H2[NHCOC(C6H4-t-Bu)3]2}2]-4(toluene)-3(CH3CN)-H2O |
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Formula | C190 H247 N9 O6 S4 W |
Calculated formula | C190 H245 N9 O5.9801 S4 W |
Title of publication | Behavior of anionic molybdenum(iv, vi) and tungsten(iv, vi) complexes containing bulky hydrophobic dithiolate ligands and intramolecular NHS hydrogen bonds in nonpolar solvents. |
Authors of publication | Hasenaka, Yuki; Okamura, Taka-Aki; Tatsumi, Miki; Inazumi, Naoya; Onitsuka, Kiyotaka |
Journal of publication | Dalton transactions (Cambridge, England : 2003) |
Year of publication | 2014 |
Journal volume | 43 |
Journal issue | 41 |
Pages of publication | 15491 - 15502 |
a | 39.235 ± 0.005 Å |
b | 23.938 ± 0.003 Å |
c | 20.131 ± 0.003 Å |
α | 90° |
β | 108.061 ± 0.005° |
γ | 90° |
Cell volume | 17976 ± 4 Å3 |
Cell temperature | 200 K |
Ambient diffraction temperature | 200 K |
Number of distinct elements | 6 |
Space group number | 15 |
Hermann-Mauguin space group symbol | C 1 2/c 1 |
Hall space group symbol | -C 2yc |
Residual factor for all reflections | 0.1484 |
Residual factor for significantly intense reflections | 0.1265 |
Weighted residual factors for significantly intense reflections | 0.3199 |
Weighted residual factors for all reflections included in the refinement | 0.3323 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.109 |
Diffraction radiation wavelength | 0.71075 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
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