Information card for entry 7032202

Structure parameters

• Formula: C47 H56 O4 Pd2 Te2
• Calculated formula: C47 H56 O4 Pd2 Te2
• SMILES: c12c(cc(cc1C)C)C[Pd]1([O]=C(C)O[Pd]3(Cc4c(c(cc(c4)C)C)[Te]3c3c(cc(cc3C)C)C)[O]1C(=O)C)[Te]2c1c(cc(cc1C)C)C.c1(ccccc1)C
• Title of publication: Cyclopalladation of telluro ether ligands: synthesis, reactivity and structural characterization.
• Authors of publication: Kolay, Siddhartha; Kumar, Mukesh; Wadawale, Amey; Das, Dasarathi; Jain, Vimal K.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2014
• Journal volume: 43
• Journal issue: 42
• Pages of publication: 16056 - 16065
• a: 11.1936 ± 0.0003 Å
• b: 33.0163 ± 0.0013 Å
• c: 11.9487 ± 0.0003 Å
• α: 90°
• β: 92.641 ± 0.002°
• γ: 90°
• Cell volume: 4411.2 ± 0.2 ų
• Cell temperature: 130 ± 0.1 K
• Ambient diffraction temperature: 130 ± 0.1 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.1009
• Residual factor for significantly intense reflections: 0.0739
• Weighted residual factors for significantly intense reflections: 0.1838
• Weighted residual factors for all reflections included in the refinement: 0.2024
• Goodness-of-fit parameter for all reflections included in the refinement: 1.047
• Diffraction radiation wavelength: 1.5418 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No