Information card for entry 7032222

Structure parameters

• Formula: C184 H188 N52 O36 Pd10
• Calculated formula: C184 H188 N52 O36 Pd10
• Title of publication: Self-assembly of tri-pyrazolate linked cages with di-palladium coordination motifs.
• Authors of publication: Jiang, Xuan-Feng; Deng, Wei; Jin, Rui; Qin, Lin; Yu, Shu-Yan
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2014
• Journal volume: 43
• Journal issue: 42
• Pages of publication: 16015 - 16024
• a: 16.367 ± 0.009 Å
• b: 18.976 ± 0.009 Å
• c: 21.069 ± 0.011 Å
• α: 94.611 ± 0.012°
• β: 107.429 ± 0.014°
• γ: 95.671 ± 0.003°
• Cell volume: 6171 ± 6 ų
• Cell temperature: 160 ± 2 K
• Ambient diffraction temperature: 160 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.076
• Residual factor for significantly intense reflections: 0.0582
• Weighted residual factors for significantly intense reflections: 0.1249
• Weighted residual factors for all reflections included in the refinement: 0.1298
• Goodness-of-fit parameter for all reflections included in the refinement: 1.077
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No