Self-assembled Cu(ii) and Ni(ii) metallamacrocycles formed from 3,3,3',3'-tetrabenzyl-1,1'-aroylbis(thiourea) ligands: DNA and protein binding studies, and cytotoxicity of trinuclear complexes.
Authors of publication
Selvakumaran, Nagamani; Bhuvanesh, Nattamai S. P.; Karvembu, Ramasamy
Journal of publication
Dalton transactions (Cambridge, England : 2003)
Year of publication
2014
Journal volume
43
Journal issue
43
Pages of publication
16395 - 16410
a
9.66 ± 0.004 Å
b
10.747 ± 0.005 Å
c
10.981 ± 0.005 Å
α
81.433 ± 0.005°
β
68.491 ± 0.005°
γ
84.688 ± 0.005°
Cell volume
1047.9 ± 0.8 Å3
Cell temperature
150 ± 2 K
Ambient diffraction temperature
150 ± 2 K
Number of distinct elements
5
Space group number
2
Hermann-Mauguin space group symbol
P -1
Hall space group symbol
-P 1
Residual factor for all reflections
0.0448
Residual factor for significantly intense reflections
0.0394
Weighted residual factors for significantly intense reflections
0.1039
Weighted residual factors for all reflections included in the refinement
0.1089
Goodness-of-fit parameter for all reflections included in the refinement
