Information card for entry 7032257

Structure parameters

• Formula: C63 H73 Au B Cl F15 Li N2 O4
• Calculated formula: C63 H73 Au B Cl F15 Li N2 O4
• Title of publication: Anionic N-heterocyclic carbenes (NHCs): a versatile route to saturated NHCs bearing pendant weakly coordinating anions.
• Authors of publication: Phillips, Nicholas; Tirfoin, Rémi; Aldridge, Simon
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2014
• Journal volume: 43
• Journal issue: 41
• Pages of publication: 15279 - 15282
• a: 10.8473 ± 0.0003 Å
• b: 16.4395 ± 0.0004 Å
• c: 19.8987 ± 0.0004 Å
• α: 69.27 ± 0.002°
• β: 87.964 ± 0.002°
• γ: 88.679 ± 0.002°
• Cell volume: 3316.39 ± 0.15 ų
• Cell temperature: 150 K
• Ambient diffraction temperature: 150 K
• Number of distinct elements: 9
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1159
• Residual factor for significantly intense reflections: 0.0839
• Weighted residual factors for all reflections: 0.2188
• Weighted residual factors for significantly intense reflections: 0.2025
• Weighted residual factors for all reflections included in the refinement: 0.2188
• Goodness-of-fit parameter for all reflections included in the refinement: 1.0183
• Diffraction radiation wavelength: 1.5418 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No