Information card for entry 7032283

Structure parameters

• Formula: C12 H18 Cl3 N3 O6.5 Ru
• Calculated formula: C12 H8 Cl3 N3 O6.5 Ru
• Title of publication: Formation of bis(2-pyridylcarbonyl)aminate by oxidation of ethylbis(2-pyridylmethyl)amine on the trichloridoruthenium(iii) complex.
• Authors of publication: Nagao, Hirotaka; Shimura, Naoto; Yonezawa, Haruka
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2014
• Journal volume: 43
• Journal issue: 41
• Pages of publication: 15391 - 15397
• a: 10.139 ± 0.004 Å
• b: 8.711 ± 0.004 Å
• c: 21.25 ± 0.008 Å
• α: 90°
• β: 96.7949 ± 0.0015°
• γ: 90°
• Cell volume: 1863.6 ± 1.3 ų
• Cell temperature: 93 K
• Ambient diffraction temperature: 93 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for significantly intense reflections: 0.0352
• Weighted residual factors for all reflections included in the refinement: 0.0794
• Goodness-of-fit parameter for all reflections included in the refinement: 1.117
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No