Information card for entry 7032508

Structure parameters

• Chemical name: 6
• Formula: C20 H18 Br2 O5 Re2 Si
• Calculated formula: C20 H18 Br2 O5 Re2 Si
• Title of publication: Synthesis and structures of doubly-bridged dicyclopentadienyl dinuclear rhenium complexes, and their photochemical reactions with aromatic halides in benzene.
• Authors of publication: Zhu, Bolin; Huang, Xinwei; Hao, Xiaoting
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2014
• Journal volume: 43
• Journal issue: 44
• Pages of publication: 16726 - 16736
• a: 13.0866 ± 0.0014 Å
• b: 14.1531 ± 0.0016 Å
• c: 13.5893 ± 0.0015 Å
• α: 90°
• β: 113.256 ± 0.002°
• γ: 90°
• Cell volume: 2312.5 ± 0.4 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0483
• Residual factor for significantly intense reflections: 0.0437
• Weighted residual factors for significantly intense reflections: 0.096
• Weighted residual factors for all reflections included in the refinement: 0.098
• Goodness-of-fit parameter for all reflections included in the refinement: 1.164
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No