Information card for entry 7032529

Structure parameters

• Formula: C127.5 H167.5 Cl4 Si16 Sn4
• Calculated formula: C127.5 H167.5 Cl4 Si16 Sn4
• Title of publication: Si(SiMe3)2SiPh3 - a ligand for novel sub-valent tin cluster compounds.
• Authors of publication: Klink, R.; Schrenk, C.; Schnepf, A.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2014
• Journal volume: 43
• Journal issue: 42
• Pages of publication: 16097 - 16104
• a: 17.0858 ± 0.0012 Å
• b: 18.5269 ± 0.0012 Å
• c: 24.0591 ± 0.0015 Å
• α: 75.208 ± 0.002°
• β: 89.665 ± 0.002°
• γ: 70.392 ± 0.002°
• Cell volume: 6909.7 ± 0.8 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0919
• Residual factor for significantly intense reflections: 0.052
• Weighted residual factors for significantly intense reflections: 0.1086
• Weighted residual factors for all reflections included in the refinement: 0.1275
• Goodness-of-fit parameter for all reflections included in the refinement: 1.014
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No