Information card for entry 7032626

Structure parameters

• Formula: C22 H43 N5 O Si2 Zn
• Calculated formula: C22 H43 N5 O Si2 Zn
• Title of publication: Enantiopure N,N,O-scorpionate zinc amide and chloride complexes as efficient initiators for the heteroselective ROP of cyclic esters.
• Authors of publication: Honrado, Manuel; Otero, Antonio; Fernández-Baeza, Juan; Sánchez-Barba, Luis F; Garcés, Andrés; Lara-Sánchez, Agustín; Rodríguez, Ana M
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2014
• Journal volume: 43
• Journal issue: 45
• Pages of publication: 17090 - 17100
• a: 12.364 ± 0.0015 Å
• b: 15.67 ± 0.0019 Å
• c: 15.71 ± 0.002 Å
• α: 90°
• β: 112.72 ± 0.007°
• γ: 90°
• Cell volume: 2807.5 ± 0.6 ų
• Cell temperature: 230 ± 2 K
• Ambient diffraction temperature: 230 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.1549
• Residual factor for significantly intense reflections: 0.1116
• Weighted residual factors for significantly intense reflections: 0.268
• Weighted residual factors for all reflections included in the refinement: 0.2897
• Goodness-of-fit parameter for all reflections included in the refinement: 1.128
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No