Information card for entry 7032638

Structure parameters

• Formula: C20 H22 Cl Co N6 O7 S4
• Calculated formula: C18 H12 Cl Co N6 O4 S4
• Title of publication: Unprecedented metal-mediated in situ reactions of heterocyclic disulfide of di[4-(pyridin-2-yl)pyrimidinyl]disulfide.
• Authors of publication: Zhu, Hai-Bin; Wu, Yan-Fang; Zhao, Yue; Hu, Jun
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2014
• Journal volume: 43
• Journal issue: 45
• Pages of publication: 17156 - 17162
• a: 18.573 ± 0.016 Å
• b: 18.573 ± 0.016 Å
• c: 31.35 ± 0.05 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 10814 ± 2 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 7
• Space group number: 87
• Hermann-Mauguin space group symbol: I 4/m
• Hall space group symbol: -I 4
• Residual factor for all reflections: 0.1386
• Residual factor for significantly intense reflections: 0.1186
• Weighted residual factors for significantly intense reflections: 0.2553
• Weighted residual factors for all reflections included in the refinement: 0.2626
• Goodness-of-fit parameter for all reflections included in the refinement: 1.187
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No