Information card for entry 7032669

Structure parameters

• Formula: C31.25 H33 Gd N5 Ni O16.25
• Calculated formula: C31.25 H33 Gd N5 Ni O16.25
• Title of publication: Probing the magnetic and magnetothermal properties of M(ii)-Ln(iii) complexes (where M(ii) = Ni or Zn; Ln(iii) = La or Pr or Gd).
• Authors of publication: Ahmed, Naushad; Das, Chinmoy; Vaidya, Shefali; Srivastava, Anant Kumar; Langley, Stuart K.; Murray, Keith S.; Shanmugam, Maheswaran
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2014
• Journal volume: 43
• Journal issue: 46
• Pages of publication: 17375 - 17384
• a: 11.286 ± 0.003 Å
• b: 26.99 ± 0.008 Å
• c: 12.817 ± 0.004 Å
• α: 90°
• β: 98.722 ± 0.005°
• γ: 90°
• Cell volume: 3859 ± 2 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0806
• Residual factor for significantly intense reflections: 0.0727
• Weighted residual factors for significantly intense reflections: 0.1829
• Weighted residual factors for all reflections included in the refinement: 0.1948
• Goodness-of-fit parameter for all reflections included in the refinement: 1.136
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No