Synthesis, structure and reactivity study of magnesium amidinato complexes derived from carbodiimides and N,N'-bis(2,6-diisopropylphenyl)-1,4-diaza-butadiene ligands.
Authors of publication
Anga, Srinivas; Bhattacharjee, Jayeeta; Harinath, Adimulam; Panda, Tarun K.
Journal of publication
Dalton transactions (Cambridge, England : 2003)
Year of publication
2015
Journal volume
44
Journal issue
3
Pages of publication
955 - 965
a
11.569 ± 0.005 Å
b
12.971 ± 0.005 Å
c
16.674 ± 0.005 Å
α
100.146 ± 0.005°
β
93.771 ± 0.005°
γ
100.24 ± 0.005°
Cell volume
2411.6 ± 1.6 Å3
Cell temperature
120 ± 2 K
Ambient diffraction temperature
120 ± 2 K
Number of distinct elements
4
Space group number
2
Hermann-Mauguin space group symbol
P -1
Hall space group symbol
-P 1
Residual factor for all reflections
0.0903
Residual factor for significantly intense reflections
0.0925
Weighted residual factors for significantly intense reflections
0.1705
Weighted residual factors for all reflections included in the refinement
0.2408
Goodness-of-fit parameter for all reflections included in the refinement
