Information card for entry 7033067

Structure parameters

• Formula: C18 H29 Ca Cl N0 O2 Si0
• Calculated formula: C18 H29 Ca Cl O2
• Title of publication: Unprecedented silicon(II)→calcium complexes with N-heterocyclic silylenes.
• Authors of publication: Blom, Burgert; Klatt, Günter; Gallego, Daniel; Tan, Gengwen; Driess, Matthias
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2015
• Journal volume: 44
• Journal issue: 2
• Pages of publication: 639 - 644
• a: 9.0963 ± 0.0006 Å
• b: 13.5005 ± 0.0009 Å
• c: 17.6543 ± 0.0013 Å
• α: 80.412 ± 0.006°
• β: 76.114 ± 0.006°
• γ: 70.938 ± 0.006°
• Cell volume: 1980.1 ± 0.3 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0653
• Residual factor for significantly intense reflections: 0.0504
• Weighted residual factors for significantly intense reflections: 0.1267
• Weighted residual factors for all reflections included in the refinement: 0.1379
• Goodness-of-fit parameter for all reflections included in the refinement: 1.103
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No