Information card for entry 7033268

Structure parameters

• Formula: C22 H38 B10 Cl N Rh S
• Calculated formula: C22 H38 B10 Cl N Rh S
• Title of publication: Metal-induced B-H bond activation: reactions between half-sandwich Ir and Rh complexes with carboranylthioamide.
• Authors of publication: Xu, Bin; Wang, Yin-Ping; Yao, Zi-Jian; Jin, Guo-Xin
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2015
• Journal volume: 44
• Journal issue: 4
• Pages of publication: 1530 - 1533
• a: 9.557 ± 0.002 Å
• b: 28.87 ± 0.007 Å
• c: 10.398 ± 0.002 Å
• α: 90°
• β: 95.087 ± 0.004°
• γ: 90°
• Cell volume: 2857.6 ± 1.1 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.1336
• Residual factor for significantly intense reflections: 0.0758
• Weighted residual factors for significantly intense reflections: 0.1825
• Weighted residual factors for all reflections included in the refinement: 0.2136
• Goodness-of-fit parameter for all reflections included in the refinement: 1.073
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No