Information card for entry 7033271

Structure parameters

• Formula: C20 H66 Cs4 O37 Rh2 Ta6
• Calculated formula: C20 H30 Cs4 O37 Rh2 Ta6
• Title of publication: Grafting {Cp*Rh}(2+) on the surface of Nb and Ta Lindqvist-type POM.
• Authors of publication: Abramov, P. A.; Sokolov, M. N.; Virovets, A. V.; Floquet, S.; Haouas, M.; Taulelle, F.; Cadot, E.; Vicent, C.; Fedin, V. P.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2015
• Journal volume: 44
• Journal issue: 5
• Pages of publication: 2234 - 2239
• a: 9.5851 ± 0.001 Å
• b: 10.5155 ± 0.0011 Å
• c: 14.6458 ± 0.0015 Å
• α: 95.814 ± 0.003°
• β: 99.365 ± 0.003°
• γ: 98.708 ± 0.003°
• Cell volume: 1427.7 ± 0.3 ų
• Cell temperature: 150 ± 0.2 K
• Ambient diffraction temperature: 150 ± 0.2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0738
• Residual factor for significantly intense reflections: 0.0481
• Weighted residual factors for significantly intense reflections: 0.0937
• Weighted residual factors for all reflections included in the refinement: 0.1061
• Goodness-of-fit parameter for all reflections included in the refinement: 1.034
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No